[Back to Contents Page] [Back to Home Page]

 

Medicinal Chemistry Reviews - Online, Volume 1, No. 1, 2004

 

Contents

 

The Use of Auxiliary Agents to Improve the Mucosal Uptake of Peptides Pp.1-10

Andreas Bernkop-Schnurch, Andreas E. Clausen  and Davide Guggi

[Abstract]

 

The Role of CD8+ T Cell Soluble Factors in Human Immunodeficiency Virus Infection: An Update Pp.11-12

Karen F.T. Copeland

[Abstract]

 

Update to Medicinal Chemistry of Nicotinamide in the Treatment of Ischemia and Reperfusion Pp.13-17

J. Yang, K. Klaidman and J.D. Adams

[Abstract]

 

Oxidative Stress Mechanisms and Potential Therapeutic Modalities in Alzheimer Disease Pp.19-23

Adam D. Cash, Mark A. Smith and George Perry

[Abstract]

 

Novel Therapeutic Targets for Acute Pancreatitis and Associated Multiple Organ Dysfunction Syndrome: An Update Pp.25-26

M. Bhatia

[Abstract]

 

Scintigraphic Imaging of Inflammatory Processes Pp.27-38

Huub J.J.M. Rennen, Otto C. Boerman, Wim J.G. Oyen and Frans H.M. Corstens

[Abstract]

 

ETS Proteins and MMPs: Partners in Invasion and Metastasis Pp.39-46

Sadmeet Singh, Jane Barrett, Kenji Sakata, Richard G. Tozer and Gurmit Singh

[Abstract]

 

Fluorinated Anthracyclines: Synthesis and Biological Activity Pp.47-71

Giuseppe Giannini

[Abstract]

 

Selective PGHS-2 Inhibitors: A Rational Approach for Treatment of the Inflammation Pp.73-90

C.R. Rodrigues, M.P. Veloso, H. Verli, C.A.M. Fraga, A.L.P. Miranda  and E. J. Barreiro

[Abstract]

 

GABA-A Receptor Complex and Memory Processes Pp.91-99

Georges Chapouthier  and Patrice Venault

[Abstract]

 

The Effects of Drugs Used in Anaesthesia on Platelet Membrane Receptors and on Platelet Function Pp.101-110

Sibylle A. Kozek-Langenecker

[Abstract]

 

Abstracts

 

[Back to top] The Use of Auxiliary Agents to Improve the Mucosal Uptake of Peptides

Andreas Bernkop-Schnurch, Andreas E. Clausen  and Davide Guggi

 

The mucosal administration of peptide drugs causes a therapeutical response only if significant amounts of the drug are enabled to permeate the absorption membrane based on the mucus layer (I) and the epithelial tissue (II) .The peptide drug transport across the membrane can be improved by the use of mucolytic agents and of permeation enhancers. The generation of novel, more potent permeation enhancers, based on a more exact knowledge of the absorption membrane in combination with appropriate delivery systems strongly improves the bioavailability of mucosally applied peptide drugs.

 

[Back to top] The Role of CD8+ T Cell Soluble Factors in Human Immunodeficiency Virus Infection: An Update

Karen F.T. Copeland

 

CD8+ T cells are strong mediators of antiviral responses. In addition to lysis of HIV infected cells, CD8+ T cells produce proteins which inhibit HIV replication by non-lytic mechanisms. These proteins include b-chemokines which inhibit viral entry and IL-16 which inhibits HIV transcription. The CD8+ T cell antiviral factor (CAF) also inhibits HIV transcription. CAF remains unidentified. This update summarizes the research conducted over the last two years pertaining to CD8+ T cell antiviral activity.

 

[Back to top] Update to Medicinal Chemistry of Nicotinamide in the Treatment of Ischemia and Reperfusion

J. Yang, K. Klaidman and J.D. Adams

 

Nicotinamide and its analogs are currently being used or investigated for the treatment of ischemia reperfusion conditions.  Nicorandil has been investigated for use in cardiac ischemia and reperfusion and is approved for use in Europe and Japan in angina.  Nicotinamide has been extensively investigated in animal models of stroke, including middle cerebral artery occlusion and spontaneously hypertensive rats.  Dose response curves and time response curves have been produced for nicotinamide in these models.  Nicotinamide spares ATP by increasing NAD levels and protecting DNA from fragmentation.  Inhibitors of poly(ADP-ribose) polymerase, including nicotinamide, have been investigated in ischemia reperfusion conditions in other organs such as the testicles and liver.  New evidence suggests that nicotinamide may have other mechanisms of action involving the regulation of cellular processes.

 

[Back to top] Oxidative Stress Mechanisms and Potential Therapeutic Modalities in Alzheimer Disease

Adam D. Cash, Mark A. Smith and George Perry

 

Alzheimer disease is characterized by oxidative damage to every class of biological macromolecule. Disruptions in iron and copper homeostasis are implicated as having key roles in neurodegenerative disease pathogenesis. Metal homeostasis as it pertains to alterations in brain function and its relation to oxidative stress in neurodegenerative diseases is reviewed here. While there is documented evidence for alterations in transition metal metabolism, redox-activity and localization, it is important to note that alterations in specific copper- and iron-containing metalloenzymes contribute to the neurodegeneration in AD. Understanding these changes offers the opportunity to identify pathways where modification of the disease process can offer effective clinical intervention, from gene therapy to pharmaceuticals with antioxidant and chelating properties.

 

[Back to top] Novel Therapeutic Targets for Acute Pancreatitis and Associated Multiple Organ Dysfunction Syndrome: An Update

M. Bhatia

 

In an article published in Current Drug Targets – Inflammation and Allergy in December 2002, I had reviewed the critical role played by inflammatory mediators in the pathogenesis of acute pancreatitis and associated multiple organ dysfunction syndrome (MODS) and the potential for these mediators as therapeutic targets. Recent work, by us as well as other investigators, has further substantiated a potential for these mediators as therapeutic targets for this condition.

 

[Back to top] Scintigraphic Imaging of Inflammatory Processes

Huub J.J.M. Rennen, Otto C. Boerman, Wim J.G. Oyen and Frans H.M. Corstens

 

Nuclear medicine offers ideal techniques to visualize inflammatory processes using noninvasive methods of whole-body scanning, enabling the determination of both the localization and the number of inflammatory foci. In nuclear medicine, a radiolabeled compound is injected (mostly) intravenously and accumulates in the inflammatory lesion due to the locally changed physiological condition. These changes are enhanced blood flow, enhanced vascular permeability and enhanced influx of leukocytes. Radiopharmaceuticals can be primarily divided into two classes: those accumulating in the inflammatory lesion based on non-specific processes and those accumulating in connection to leukocytes. Nonspecific tracers like 67Ga-citrate, radiolabeled non-specific immunoglobulins and radiolabeled liposomes are discussed in detail. Studies using specific tracers mainly focus on radiolabeling leukocytes, either directly or indirectly. Direct labeling of isolated leukocytes and reinjecting them is considered the “gold standard” nuclear medicine technique for imaging inflammation. Labeling leukocytes in vivo (the indirect approach) can be achieved by the use of radiolabeled antibodies or by compounds binding to leukocyte receptors with high affinity. At least three anti-granulocyte antibodies have been tested for infection imaging: anti-NCA-95 IgG (BW250/183), anti-NCA-90 Fab' (Immu-MN3, leukoscan®: anti-CD66), and anti-SSEA-1 IgM (LeuTech®: anti-CD15). In addition, a wide variety of peptides binding to leukocyte receptors has been investigated, e.g. chemotactic peptide formyl-Met-Leu-Phe, cytokines such as interleukin-1, interleukin-2, interleukin-8 and platelet factor 4 (derivatives) and complement factors such as C5a. Furthermore, positron emission tomography with 18F-fluorodeoxyglucose takes advantage of the enhanced glucose requirements of leukocytes and macrophages in inflammatory foci. A totally different approach is to target directly micro-organisms, without intervention of leukocytes. This strategy is adopted in radiopharmaceuticals such as Infecton and antimicrobial peptides. The discussed radiopharmaceuticals enable accurate diagnosis of the inflammatory condition and with these agents the effectiveness of anti-inflammatory therapies can be monitored.

 

[Back to top] ETS Proteins and MMPs: Partners in Invasion and Metastasis

Sadmeet Singh, Jane Barrett, Kenji Sakata, Richard G. Tozer and Gurmit Singh

 

Binding sites for the ETS domain family of transcription factors are found in the promoters of the matrix metalloproteinase (MMP) family of matrix degrading enzymes. Evidence is accumulating that both these groups of molecules are important in the process of angiogenesis in addition to matrix degradation. Furthermore, they are both expressed in tumor tissue as well as in the normal surrounding stroma. These factors along with various sites at which they may be regulated collectively makes them attractive targets to consider for therapeutic intervention in the processes of invasion and metastasis.

 

[Back to top] Fluorinated Anthracyclines: Synthesis and Biological Activity

Giuseppe Giannini

 

Organic structures with fluorine atom are slightly diffuse in nature.

 

Starting ‘80s researchers have discovered that the selective introduction of fluorine into biologically active molecules exercised an influence on activity. So an important endeavour in drug design have been described and numerous compounds incorporating fluorine as either a bioisosteric replacement for hydrogen or an isoelectronic replacement for the hydroxyl group have been reported.

 

Parallely, an enormous literature on anthracyclines exists, a class of compounds used in clinical since ‘70s, as antitumor drugs. Unfortunately, the anthracyclines are known as well for several toxical effects that frequently condition the clinical use.

 

In the last decade a lot of anthracycline derivatives has been described in which has been introduced a fluorine atom in different position of molecule.

 

This review wishes to represent an updated collection of compounds with anthracycline structure where a fluorine atom has been introduced on aglycon or/and sugar moiety.

 

Together with the chemical structures, the synthetic indications are furnished and succinct explanations of biological activity are summarised (if available).

 

[Back to top] Selective PGHS-2 Inhibitors: A Rational Approach for Treatment of the Inflammation

C.R. Rodrigues, M.P. Veloso, H. Verli, C.A.M. Fraga, A.L.P. Miranda  and E. J. Barreiro

 

Prostaglandin-H synthase exists in two isoforms, PGHS-1 and PGHS-2. PGHS-1 is present and is constitutively expressed in most cells and tissues, whereas PGHS-2 is mainly thought to mediate inflammation. Selective prostaglandin-H synthase-2 (or cyclooxygenase-2)  inhibitors have been shown to be potent antiinflammatory agents with fewer side effects than currently marketed nonsteroidal antiinflammatory drugs (NSAIDs). This review addresses the main classes of the selective PGHS-2 inhibitors whose selectivity is documented by supporting PGHS-1 and PGHS-2 enzyme data. In addition, we also describe our experience in design, synthesis and pharmacological in vivo evaluation of new 1,2-benzodioxole derivatives as candidate of the selective PGHS-2 inhibitors, with special attention to molecular dynamics simulations of these derivatives attached to the active site of PGHS-2.

 

[Back to top] GABA-A Receptor Complex and Memory Processes

Georges Chapouthier  and Patrice Venault

 

Considerable evidence has been provided these last years for the involvement of the GABAA receptor complex in memory processes. Compounds that enhance the action of GABA, such as benzodiazepines, impair memory processing. On the contrary, compounds that reduce the action of GABA, such as ß-CCM, pentylenetetrazol or picrotoxin, have the opposite action, that is : enhance memory processing. All these actions seem to focus mainly on the acquisition (learning) processes. Depending on the dose, the same compounds also have effects on anxiety and on seizuring. Benzodiaze-pines  are  well-known  anxiolytic  and  anticonvulsant  agents  whereas  compounds  that reduce the action of GABA have been found to produce anxiogenic and convulsant actions. The GABAA receptor complex might thus be the location of a possible link between a pathological state (epilepsy) and two normal functions (anxiety and learning). This link is likely to involve common genetic pathways. In the normal subject, these data also emphasize the idea that normal memory processing involves a moderate level of anxiety.

 

[Back to top] The Effects of Drugs Used in Anaesthesia on Platelet Membrane Receptors and on Platelet Function

Sibylle A. Kozek-Langenecker

 

Platelet dysfunctions are known origins of perioperative bleeding disorders which are a major concern in the management of surgical patients. Among multiple factors, interactions of drugs used in anaesthesia with platelets have been implicated to aggravate the risk of haemorrhagic complications. This paper reviews in vitro and in vivo studies which have examined the effects of inhalational, intravenous, and local anaesthetics, opioids, and muscle relaxants on platelets. A brief summary of platelet physiology, function tests, and flow cytometric assessment of membrane receptors is included. Although the results of many studies have been conflicting, it appears that halothane, sevoflurane, and propofol inhibit platelet function in a reversible and dose-related manner at concentrations used clinically. Halothane affects the intracellular activating second messenger inositol triphosphate, platelet calcium homeostasis, thromboxane A2 formation, and the inhibiting signal transduction pathway including cyclic adenosine monophosphate. The proposed platelet inhibiting mechanism of sevoflurane involves the suppression of thromboxane A2 formation. Propofol appears to cause platelet dysfunctions by inhibiting calcium mobilisation upon agonist stimulation. Nitrous oxide causes a modest suppression of calcium mobilisation. An interaction of local anaesthetics with components in the platelet membrane appears to account for their inhibiting effect, but only at concentrations far higher than that found during clinical use. A clinically relevant antithrombotic effect of regional anaesthesia has been observed, though. Isoflurane, enflurane, desflurane, barbiturates, etomidate, opioids, and muscle relaxants seem to have negligible effects on platelets at therapeutic concentrations. Anaesthetists should be aware of the potential impairment of the coagulation profile by anaesthetic agents.